Periodicity behavior was observed after droplet collision in viscous solutions with controlled glycerol concentrations onto a PDMS surface. No periodic movement was observed in the droplets at glycerol concentrations of 50% or more. In contrast, the vertical diameter of the droplets increased and decreased periodically at glycerol solution concentrations of 40% or less. Moreover, there was little change in the periodicity of the impacting droplet movement, and the vibration frequency was measured at approximately 80 to 98 Hz in the entire range. The maximum droplet spreading factor after collision decreased significantly with increasing glycerol concentrations of 40% or more (Ohnesorge number 1.4 × 10-2 or more). The results suggest that the effect of viscosity became greater than that of the solution surface tension with increasing glycerol concentrations.
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To monitor the stirring state by on-line estimation of liquid viscosity instead of stopping the stirring process and measuring the viscosity using viscometer, a basic study clarifying the effect of stirring conditions was carried out. For this purpose, the relationship between liquid viscosity and the stirring conditions, such as stirring torque, stirring speed, the duty ratio of PWM, impeller and beaker type, and the blade position in the beaker was analyzed. The second-order relationship between the stirring speed and torque, the linear relationship between viscosity and torque, and the linear relationship between duty ratio of PWM and stirring speed were observed, thereby indicating that the liquid viscosity could be estimated by an experimental formula based on the duty ratio and the stirring speed. In addition, the type of impeller and beaker was identified using the magnetic field inside impeller and RFID technology. For reducing the error in calculating the liquid viscosity, the employment of an impeller blade with a large rotational resistance and stirring with the blade at the center zone of the beaker were found to be necessary.
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Since most commercialized DLP 3D printers fabricate 3D structures by sinking materials to Vat using a bottom-up method, it is difficult to use various materials simultaneously and there are many restrictions on printing composite materials. Especially, composite resin mixed with various functional powders in photo curable resin generally has high viscosity, causing difficult material flow in the bottom-up method when using Vat. Additionally, most of the previously presented methods for fabricating multi-material structure use individual curing for each material, so the adhesion force at the contact surface is less than 50% compared to single material. Thus, in this paper, we propose a new type of DLP 3D printer that combines Material Extrusion and the DLP system. The proposed equipment can supply high viscosity composite material resins to a specific area to cure various materials simultaneously. This method will enable fabrication of multiple composite material structures with sufficient adhesion force. The tensile test will be performed to verify suitability of the proposed method.
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